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In-depth video instructions on how to set up your copy of TopSolid and. click to download the zip file and install. .Photoacoustic calorimetry.
We present a photoacoustic calorimeter for the in situ measurement of thermodynamic properties of condensed matter systems, such as the latent heat of vaporization and the enthalpy of evaporation of liquids. The device consists of a cubic cavity with windows at the top and at the bottom. A pulsed focused laser light pulse is directed through the top window to heat a sample and simultaneously through the bottom window to the surrounding thermo-electric cooler. The resulting temperature difference is measured as a voltage using a high temperature metal-oxide resistor and a lock-in amplifier. In the prototype the laser light pulse and cooling steps are computer-controlled. The power of our device is limited by the temperature difference and the temperature gradient between the sample and the surrounding liquid. We demonstrate the reproducibility of the liquid evaporation process with a trapped and thermally isolated sample of liquid water at room temperature. A volume of 33 μL of liquid can be evaporated in 12 s, yielding a reproducibility of the latent heat of water evaporation of 7 mJ.Monday, April 30, 2009
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